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Beilstein J. Org. Chem. 2012, 8, 1849–1857, doi:10.3762/bjoc.8.213
Graphical Abstract
Scheme 1: Synthesis of ethyl 2-(chloromethyl)-4-phenylquinoline-3-carboxylate (2).
Scheme 2: Synthesis of 2-(phenoxymethyl)-4-phenylquinoline-3-carboxylic acid derivatives 3a–l.
Scheme 3: Synthesis of 12-phenylbenzo[6,7]oxepino[3,4-b]quinolin-13(6H)-ones 4a–h.
Scheme 4: Cyclization and de-tert-butylation reaction of 3l by using PPA.